Gas Chromatographic Analysis

Description

Analytical Methods for Pesticides and Plant Growth Regulators, Volume VI: Gas Chromatographic Analysis covers the topics pesticide analyses by gas chromatography. The book discusses the sample preparation, detectors, qualitative analyses, and formulation analyses, as well as gas chromatography of different classes of pesticides. The text also provides general information concerning specific insecticides, fungicides, herbicides, plant growth regulators, nematicides and soil fumigants, as well as analytical techniques other than gas chromatography. Toxicologists and people involved in agricultural research will find the book invaluable.

Front Cover 2
Gas Chromatographic Analysis 5
Copyright Page 6
Table of Contents 7
Contributors to Volume VI 25
Preface 27
PART I: GENERAL 29
- Chapter 1. Sample Preparation 31
  - I. Sampling for Pesticide Residue Analysis 31
  - II. Cleanup and Extraction 39
  - III. Derivative Formation 59
  - References 67
- Chapter 2. Detectors for Gas Chromatography of Pesticides 69
  - I. Emission Detectors 69
  - II. Thermionic Alkali Flame Ionization Detector 84

Front Cover 2
Gas Chromatographic Analysis 5
Copyright Page 6
Table of Contents 7
Contributors to Volume VI 25
Preface 27
PART I: GENERAL 29
- Chapter 1. Sample Preparation 31
  - I. Sampling for Pesticide Residue Analysis 31
  - II. Cleanup and Extraction 39
  - III. Derivative Formation 59
  - References 67
- Chapter 2. Detectors for Gas Chromatography of Pesticides 69
  - I. Emission Detectors 69
  - II. Thermionic Alkali Flame Ionization Detector 84
  - III. Electrochemical Detectors 90
  - IV. Electron Capture Detector 100
  - V. Summary 101
  - References 103
- Chapter 3. Qualitative Analysis of Pesticides 107
  - II. Identification Based on Retention Time 107
  - I. Introduction 107
  - III. Identification Based on Specific Detectors 113
  - IV. Identification of Multiple Insecticide Residues 114
  - V. Correlation of Molecular Structure and Electron-Capturing Ability 116
  - VI. Carbon Skeleton Chromatography 117
  - VII. Fragmentation Procedures 118
  - VIII. Extraction p-Values 119
  - IX. Gas Chromatography Combined with Thin-Layer Chromatography 124
  - X. Combination of Gas Chromatography with Other Instrumental Techniques 125
  - References 133
- Chapter 4. Formulation Analysis 137
  - I. Introduction 137
  - II. Instrumental Aspects 137
  - III. Internal Standard Technique 145
  - IV. Composition and Analysis of Formulations 152
  - V. Comparison Between GLC and Classical Methods 158
  - References 160
- Chapter 5. Chlorinated Pesticides 162
  - I. Sample Preparation 162
  - II. Detectors 185
  - III. Instrumentation and Techniques 187
  - IV. Chromatographic Systems and Data 194
  - V. Qualitative Analysis 214
  - References 216
  - VI. Applications 216
- Chapter 6. Organophosphate Pesticides 221
  - I. Sample Preparation 221
  - II. Detectors 233
  - III. Chromatographic Systems and Data 236
  - IV. Identification of Pesticides 241
  - V. Applications 257
  - References 261
- Chapter 7. Miscellaneous Classes of Pesticides 264
  - I. Sulfur Compounds 264
  - II. Nitrogen–Containing Pesticides 266
  - III. Other Classes of Pesticides 286
  - IV. Multiclass Residues 294
  - References 295
- PART II: INSECTICIDES 299
  - Chapter 8. Aldrin and Dieldrin 300
    - I. General 300
    - II. Analysis 300
  - Chapter 9. Allethrin 315
    - I. General 315
    - II. Analysis 315
    - References 316
  - Chapter 10. Aramite 317
    - II. Residue Analysis 317
    - I. General 317
    - References 318
  - Chapter 11. Azodrin® Insecticide and Bidrin® Insecticide 319
    - I. General 319
    - II. Analysis 319
  - Chapter 12. Banol 331
    - I. General 331
    - II. Analysis 331
    - References 332
  - Chapter 13. Baytex 333
    - II. Analysis 333
    - I. General 333
    - References 345
  - Chapter 14. Binapacryl 346
    - References 346
    - I. General 346
    - II. Analysis 346
  - Chapter 15. Chlordane 347
    - II. Analysis 347
    - I. General 347
    - References 350
  - Chapter 16. Chlorobenzilate 351
    - III. Residue Analysis 351
    - I. General 351
    - II. Formulation Analysis 351
    - References 353
  - Chapter 17. Chlorthion 354
    - I. General 354
    - II. Residue Analysis 354
    - References 356
  - Chapter 18. Ciodrin® Insecticide 357
    - II. Analysis 357
    - I. General 357
  - Chapter 19. Co–Ral (Coumaphos) 364
    - II. Analysis 364
    - I. General 364
    - References 371
  - Chapter 20. DDT 372
    - I. General 372
    - II. Residue Analysis 372
    - References 375
  - Chapter 21. Diazinon 377
    - II. Analysis 377
    - I. General 377
    - References 381
  - Chapter 22. Dibrom (Naled) 382
    - I. General 382
    - II. Analysis 382
    - Reference 387
  - Chapter 23. Dimetan 388
    - II. Analysis 388
    - Reference 388
    - I. General 388
  - Chapter 24. Dimethoate 389
    - I. General 389
    - II. Formulation Analysis 389
    - III. Residue Analysis 394
    - References 407
  - Chapter 25. Dimetilan 408
    - Reference 408
    - I. General 408
    - II. Analysis 408
  - Chapter 26. Di–Syston (Disulfoton; Thio–Demeton) 409
    - II. Residue Analysis 409
    - I. General 409
    - References 418
  - Chapter 27. Dylox 419
    - I. General 419
    - II. Analysis 419
    - References 423
  - Chapter 28. Endrin 425
    - II. Residue Analysis 425
    - I. General 425
    - References 426
  - Chapter 29. Ethion 428
    - References 428
    - I. General 428
    - II. Residue Analysis 428
  - Chapter 30. Guthion 429
    - II. Analysis 429
    - I. General 429
    - References 435
  - Chapter 31. Heptachlor 436
    - I. General 436
    - II. Analysis 436
    - References 439
  - Chapter 32. Imidan® 440
    - II. Formulation Analysis 440
    - I. General 440
    - III. Residue Analysis 441
    - References 445
  - Chapter 33. Isolan 446
    - II. Analysis 446
    - I. General 446
  - Chapter 34. Kelthane (Dicofol) 447
    - II. Residue Analysis 447
    - I. General 447
    - References 448
  - Chapter 35. Lethane 449
    - Reference 449
    - I. General 449
    - II. Analysis 449
  - Chapter 36. Malathion 450
    - II. Formulation Analysis 450
    - I. General 450
    - III. Residue Analysis 455
    - References 463
  - Chapter 37. Meta-Systox 464
    - II. Residue Analysis 464
    - I. General 464
    - References 472
  - Chapter 38. Methoxychlor 473
    - I. General 473
    - II. Residue Analysis 473
    - References 474
  - Chapter 39. Methyl Trithion 475
    - II. Analysis 475
    - I. General 475
  - Chapter 40. Morestan 476
    - II. Anal ysis 476
    - I. General 476
  - Chapter 41. Parathion 477
    - II. Residue Analysis—Review of Methods 477
    - I. General 477
    - References 478
  - Chapter 42. Perthane 479
    - I. General 479
    - II. Residue Analysis 479
    - Reference 480
  - Chapter 43. Phencapton 481
    - II. Residue Analysis 481
    - Reference 481
    - I. General 481
  - Chapter 44. Phosdrin® Insecticide 482
    - I. General 482
    - II. Analysis 482
  - Chapter 45. Phosphamidon 489
    - Reference 489
    - I. General 489
    - II. Residue Analysis 489
  - Chapter 46. Piperonyl Butoxide 490
    - I. General 490
    - II. Analysis 490
    - References 492
  - Chapter 47. Pyrethrins 493
    - I. General 493
    - II. Analysis 493
    - References 502
  - Chapter 48. Pyrolan 503
    - I. General 503
    - II. Analysis 503
  - Chapter 49. Rltothane (DDD) 504
    - I. General 504
    - II. Analysis 504
    - References 504
  - Chapter 50. Ronnel (Fenehlorphos) 505
    - II. Analysis 505
    - I. General 505
    - References 509
  - Chapter 51. Sevin (Carbaryl) 510
    - II. Residue Analysis 510
    - I. General 510
    - References 514
  - Chapter 52. Systox 515
    - I. General 515
    - II. Analysis 515
    - References 519
  - Chapter 53. Tedion (Tetradifon) 520
    - II. Residue Analysis 520
    - I. General 520
    - References 524
  - Chapter 54. Thimet (Phorate) 525
    - I. General 525
    - II. Formulation Analysis 525
    - III. Residue Analysis 530
    - IV. Applicability of Recommended Method to Different Crops or Commodities 541
    - References 542
  - Chapter 55. Thiodan (Endosulfan) 543
    - I. General 543
    - II. Analysis 543
    - References 544
  - Chapter 56. Toxaphene 546
    - II. Residue Analysis 546
    - I. General 546
    - References 550
  - Chapter 57. Trithion® 551
    - I. General 551
    - II. Formulation Analysis 551
    - III. Residue Analysis 553
    - References 560
  - Chapter 58. Vapona® Insecticide 561
    - I. General 561
    - II. Analysis 561
  - Chapter 59. Zectran 574
    - I. General 574
    - II. Residue Analysis 574
    - References 576
  - PART III: FUNGICIDES 577
    - Chapter 60. Actidione 579
      - I. General 579
      - II. Analysis 579
    - Chapter 61. Captan and Phaltan 580
      - I. General 580
      - II. Analysis 580
      - References 584
    - Chapter 62. Chloranil 584
      - II. Analysis 584
      - References 584
      - I. General 584
    - Chapter 63. Cyprex 585
      - I. General 585
      - II. Analysis 585
    - Chapter 64. Dexon 586
      - I. General 586
      - II. Analysis 586
    - Chapter 65. 2,6-Dichloro-4-nitroaniline (DCNA; Botran®) 587
      - II. Residue Analysis 587
      - I. General 587
      - References 589
    - Chapter 66. Difolatan® 590
      - I. General 590
      - II. Analysis 590
      - Reference 594
    - Chapter 67. Dithiocarbamates 595
      - II. Analysis 597
      - References 597
      - I. General 597
    - Chapter 68. Dyrene 598
      - I. General 598
      - II. Residue Analysis 598
      - References 600
    - Chapter 69. Glyodin 601
      - II. Analysis 601
      - I. General 601

Analytical Methods for Pesticides and Plant Growth Regulators, Vol. 6

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