Modern Analytical Techniques

Description

Analytical Methods for Pesticides and Plant Growth Regulators, Volume XIV: Modern Analytical Techniques covers an updated treatment of the most frequently used techniques for pesticide analysis, i.e., thin-layer chromatography, gas chromatography (packed and capillary columns), high-performance liquid chromatography, and mass spectrometry. People involved in the analysis of pesticides will find the book useful.

Front Cover 2
Modern Analytical Techniques 3
Copyright Page 4
Table of Contents 5
Preface 7
Chapter 1. Thin-Layer Chromatography 9
- I. INTRODUCTION 9
- II. MATERIALS AND METHODS 10
- III. RECENT APPLICATIONS OF TLC TO PESTICIDE ANALYSIS 32
- REFERENCES 43
Chapter 2. Practical Aspects of Gas Chromatography 49
- I. INTRODUCTION 49
- II. INSTRUMENTATION 50
- III. ANALYSIS 59
- REFERENCES 81

Front Cover 2
Modern Analytical Techniques 3
Copyright Page 4
Table of Contents 5
Preface 7
Chapter 1. Thin-Layer Chromatography 9
- I. INTRODUCTION 9
- II. MATERIALS AND METHODS 10
- III. RECENT APPLICATIONS OF TLC TO PESTICIDE ANALYSIS 32
- REFERENCES 43
Chapter 2. Practical Aspects of Gas Chromatography 49
- I. INTRODUCTION 49
- II. INSTRUMENTATION 50
- III. ANALYSIS 59
- REFERENCES 81
Chapter 3. Capillary Column Gas Chromatography of Pesticides 83
- II. INTRODUCTION OF SAMPLE 83
- I. INTRODUCTION 83
- III. THE CAPILLARY COLUMN 85
- IV. EXPERIMENTAL CONDITIONS 90
- V. DETECTORS 92
- VI. SPECIFIC APPLICATION OF CAPILLARY GAS CHROMATOGRAPHY 93
- REFERENCES 100
Chapter 4. High-Performance Liquid Chromatography 103
- I. INTRODUCTION 103
- II. COLUMNS 104
- III. DETECTORS 109
- IV. SAMPLE CLEANUP BY HPLC 116
- V. DERIVATIZATION 118
- VI. MULTIRESIDUE PROCEDURES 121
- VII. REPORTED METHODS OF HPLC ANALYSIS OF PESTICIDES 122
- REFERENCES 136
Chapter 5. Practical Techniques for Mass Spectrometric Analysis of Pesticides and Their Degradation Products 141
- I. INTRODUCTION 141
- II. PROCESSES AND EXPERIMENTAL TECHNIQUES 142
- III. APPLICATIONS OF MASSS PECTROMETRIC TECHNIQUES TO ANALYSIS OF PESTICIDES AND THEIR DEGRADATION PRODUCTS 160
- REFERENCES 191
- IV. CONCLUSION 191
- ACKNOWLEDGMENT 191
Chapter 6. Regulatory Pesticide Analysis by Mass Spectrometry 201
- I. INTRODUCTION 201
- II. THE ANALYTICAL APPROACH 202
- III. CASE HISTORIES 206
- IV. CONCLUSIONS 258
- REFERENCES 258
Index 263

Analytical Methods for Pesticides and Plant Growth Regulators, Vol. 14

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